5/31/2016

NECO 2016 EXPO : Practical Chemistry Questions And Answers

Today's examination papers
Tuesday 31st May.
Paper I: Practical Chemistry 10:00am – 12pm

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(A) ONE BURETTE (50cm³)
(B) ONE PIPETTE (20cm³) OR
25cm³)
NOTE:ALL CANDIDATES IN A
CENTRE MUST USE PIPETTES OF
THE SAME VOLUME.
(C) THE USUAL OF THE SAME FOR
FILTRATION
(D) THE USUAL APPARATUS AND
REAGENTS FOR QUALITATIVE
WORK INCLUDING:
(i) RED AND BLUE LITMUS PAPER
(ii) AQUEOUS AMMONIA
(iii) DILUTE HNO³-
(iv) DILUTE SILVER
TRIOXONITRATE (V)
SOLUTION
(v) AQUEOUS SODIUM
HYDROXIDE

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(vi) DILUTE HCI
(vii) POTASSIUM THIOCYNATE
SOLUTION
(viii) POTASSIUM
HEPTAOXOCHROMATE
(VII)
SOLUTION
(ix) BARIUM CHLORIDE
SOLUTION
(E) SPATULA
(F) FILTRATION APPARATUS
(G) ONE BEAKER
(H) ONE BOILING TUBE
(I) FOUR TEST TUBE
(J) PHENOLPHTHALEIN
INDICATOR
(K) METHYL ORANGE INDICATOR
(I) MATHEMATICAL TABLE/
CALCULATOR
(M) WASH BOTTLE CONTAINING
DISTILLED/ DEIONIZER WATER
Tuesday 31st may 2016
CHEMISTRY PRACTICAL 10:00am-12:00pm
+++++++++++++++++++++++++++++++++++


1)
TABULATE
Burette reading(cm^3):Final reading(cm^3),Initial reading(cm^3),Volume of acid used(cm^3)
Rough:26.00,2.00,24.00
1st reading:25.50,1.00,24.50
2nd reading:24.50,0.00,24.50
3rd reading:24.50,0.00,24.50
Average volume of acid used
=1st+2nd+3rd/3
=24.50+24.50+24.50/3
=24.50cm^3
Concentration of A mol/dm^3=Conc g/dm^3/molar mass
Molar mass of H2SO4 =2(1)+32+4(16)
=98g/dm^3
Concentration mol/dm^3=4.90/98
=0.05mol/dm^3
i)Using CaVa/CbVb=na/nb
(0.05*24.50)/Cb*25)=1/2
Cb=(0.05*24.50*2)/25
=0.098mol/dm^3
ii)Concentration of B in g/dm^3=Conc in mol/dm^3*molar mass
Molar mass of NaOH=26+16+1=40g/mol
=0.098mol/dm^3*40g/mol
=3.92g/dm^3
iii)percentage purity of B=Concentration of pure/concentration of impure *100%
=3.92/4*100%
=98%
Therefore percentage of impurity of B =100-98%
=2%


1)
volume of pipette used =25.0cm^3
indicator used =methyl orange
burette reading|rough| 21.50|0.00|21.50|
final burette readings (cm^3)|1st|21.20| 0.00. 21.20|
initial burette reading(cm^3)|2nd|31.20|10.00| 21.20|
volume of a used (cm^3)|3rd|41.20|20.00|21.20|
average volume of a used =(21.20+21.20+21.20)cm^3/3
=63.60cm^3/3
=21.20cm^3

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equation of the reaction
H2SO4(aq) + 2NaoH(aq)+2H2O(s)
nA=1,nB=2
A=4.90gldm^3 H2SO4
molar mass H2SO4
=(1*2)+32+(16*4)
=2+32+64
=98gmol^-1
molar conc A=mass con A/molar mass A
=4.90gldm^3/98glmol
=0.05moldm^3
CAVA/CBVB=nA/nB
0.05moldm^3*21.20cm^3/CB*25.0cm^3=1/2
0.05moldm^3*21.20*2=CB*25.0
CB=0.05molldm^3*21.20*2/25.0
CB=0.0848moldm^3
in mass conc B =Molar B*MolarBmass
B=NaoH
=23+16+1
=40gmol-^3
mass conc B =0.0848moldm^3 * 40gmol
mass con B = 3.392gldm^3
% mass of impusx 100%/total mass of implusty
mass of implus =(4.0-3.392)gldm^3
=0.608gldm^3
%impurity =0.608gldm^3*100%/4.0gldm^3
=15.2%
 3ai)

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Drawing lebel
-lid
-sticky tape(to hold paper)
-choroatographic paper
-gas jar
-applied spot of solute mixture
-ion
3aii)
principle of dillution, C1 V1=C2 V2
2.0molldm^3*40
3bi)
ethanol—->ethanoic (acid)—->trioxonotrate(v) (acid)
3bii)
indicators are used to determine the end point of the reaction and to test the acidity or alkalinity of a solution

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CHEMISTRY PRACTICAL ANSWERS...
2ai)
Observation:The salt sample dissolves completely
Inference:C is a mixture of soluble salts
2aii)
Observation:White precipitate insoluble in excess NaOH(aq)
Inference:Ca^2+ present
2aiii)
Observation:No visible reaction
Inference:Ca^2+ is present
2aiv)
Observation:Brownish fume is produced
Inference:NO2(g) form, NO3^- present
2av)
Observation:Formation of brown gas which forms a ring junction with FeSO4
Inference:NO2 form, NO3^- confirmed
2bi)
Observation:D dissolves completely. Formation of dirty green precipitate insoluble in excess NaOH(aq)
Inference:D is soluble in salt, Fe^2+ present
2bii)
Observation:Formation of a white precipitate.precipitate remains insoluble in HCl(aq)
Inference:SO3^2-,CO3^2-,SO4^2- present,SO4^2- confirmed

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(3ai)
Drawing lebel


-lid
-sticky tape(to hold paper)
-choroatographic paper
-gas jar
-applied spot of solute mixture
-ion
3aii)
principle of dillution, C1 V1=C2 V2
2.0molldm^3*40
3bi)
ethanol---->ethanoic (acid)---->trioxonotrate(v) (acid)
3bii)
indicators are used to determine the end point of the reaction and to test the acidity or alkalinity of a solution
1)
volume of pipette used =25.0cm^3
indicator used =methyl orange
burette reading|rough| 21.50|0.00|21.50|
final burette readings (cm^3)|1st|21.20| 0.00. 21.20|
initial burette reading(cm^3)|2nd|31.20|10.00| 21.20|
volume of a used (cm^3)|3rd|41.20|20.00|21.20|
average volume of a used =(21.20+21.20+21.20)cm^3/3
=63.60cm^3/3
=21.20cm^3
equation of the reaction
H2SO4(aq) + 2NaoH(aq)+2H2O(s)
nA=1,nB=2
A=4.90gldm^3 H2SO4
molar mass H2SO4
=(1*2)+32+(16*4)
=2+32+64
=98gmol^-1
molar conc A=mass con A/molar mass A
=4.90gldm^3/98glmol
=0.05moldm^3
CAVA/CBVB=nA/nB
0.05moldm^3*21.20cm^3/CB*25.0cm^3=1/2
0.05moldm^3*21.20*2=CB*25.0
CB=0.05molldm^3*21.20*2/25.0
CB=0.0848moldm^3
in mass conc B =Molar B*MolarBmass
B=NaoH
=23+16+1
=40gmol-^3
mass conc B =0.0848moldm^3 * 40gmol
mass con B = 3.392gldm^3
% mass of impusx 100%/total mass of implusty
mass of implus =(4.0-3.392)gldm^3
=0.608gldm^3
%impurity =0.608gldm^3*100%/4.0gldm^3
=15.2%
*note your school will give a value(end point). Your value should not be more or less than +/- 0.2 to what is being given*
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